Analysis of fracture surfaces of CF(PyC)/MgLi composites by means of in-situ Auger electron spectroscopy (in Slovak) KUDELA, S., BAUNACK, S., JOHN, A., KUDELA, S. Jr., WETZIG, K. vol. 40 (2002), no. 6, pp. 402 - 412
Abstract Composite bar made of Mg-12wt.{%}Li alloy reinforced with pyrolytic carbon coated T300 carbon fibers was broken under vacuum of 5 x 10-8 Pa in the chamber of the Auger apparatus. Both fiber jacket and fiber cross-fracture were analyzed with Auger electron spectroscopy focusing on Mg(LVV), Li(KVV), C(KVV) and O(KVV) transition regions. Thin oxidic film consisting predominantly of Li-O type compounds was found on the fiber jacket and fiber cross-fracture. After sputtering, this film almost disappeared wherein "carbidic" C(KVV) patterns belonging to Li2C2 were detected quite uniformly within whole fiber cross-fracture. Key words MgLi matrix composites, carbon fiber, Auger electron spectroscopy, lithium carbide Full text not available
|