Evolution of secondary phases in 18Cr-12Ni-3Mo steel during ageing at 650-950 °C (in Slovak) ZAHUMENSKY, P., JANOVEC, J., DOMANKOVA, M., MAGULA, V. vol. 36 (1998), no. 5, pp. 309 - 319
Abstract Changes in the microstructural stability, chemical composition, size, and morphology of secondary phases during ageing of the austenitic 17 341 steel at 650-950 °C up to 300 h are investigated in the present work. To determine above enumerated parameters, methods of light and transmission electron microscopies including EDX-analysis and electron diffraction were used. In the studied steel particles of M23C6, M6C, MX, σ, and Laves phases were identified. The triangular, square-shaped, and lath particles of the M23C6 carbide were found at grain boundaries. It was shown that the Cr/Fe ratio in particles of the same carbide increases with increasing the ageing time (temperature). The time-temperature diagram characterizing changes in size of intergranular particles during ageing was constructed. Key words microstructure, steel particles of M23C6, M6C, MX, σ, and Laves phases, ageing, austenitic 17 341 steel, EDX-analysis, electron diffraction Full text not available
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